Quantitative chemical analysis of perovskite deposition using spin coating

Peter J. Holliman; Eurig W. Jones; Robert J. Hobbs; Arthur Connell; Leo Furnell; Rosie Anthony; Christopher P. Kershaw

doi:10.1016/j.mlblux.2019.100011

Quantitative chemical analysis of perovskite deposition using spin coating

Peter J. Holliman, Eurig W. Jones, Robert J. Hobbs, Arthur Connell, Leo Furnell, Rosie Anthony, Christopher P. Kershaw

Research output: Contribution to journal › Article › peer-review

Abstract

Lead and halide ion compositions of spin coated organo-lead halide perovskite films have been quantified using ion chromatography (IC) and atomic absorption spectroscopy (AAS) using perovskite films manufactured by 5 different researchers (3 replicates per treatment) to monitor variability between researchers and individual researcher reproducibility. Planar and mesoporous TiO2-coated glass substrates have been studied along with tribromide (CH3NH3PbBr3), triiodide (CH3NH3PbI3) and mixed halide (CH3NH3PbI3−xClx) perovskite films. The data show low yields of spin coated perovskite material (ca. 1%) and preferential deposition of I− over Cl− in mixed halide films.

Original language	English
Article number	100011
Journal	Materials Letters: X
Volume	2
Early online date	1 Apr 2019
DOIs	https://doi.org/10.1016/j.mlblux.2019.100011
Publication status	Published - Jun 2019

Keywords

Solar energy materials
Thin films
Manufacturing
Perovskites
Composition

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http://www.sciencedirect.com/science/article/pii/S2590150819300353

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title = "Quantitative chemical analysis of perovskite deposition using spin coating",

abstract = "Lead and halide ion compositions of spin coated organo-lead halide perovskite films have been quantified using ion chromatography (IC) and atomic absorption spectroscopy (AAS) using perovskite films manufactured by 5 different researchers (3 replicates per treatment) to monitor variability between researchers and individual researcher reproducibility. Planar and mesoporous TiO2-coated glass substrates have been studied along with tribromide (CH3NH3PbBr3), triiodide (CH3NH3PbI3) and mixed halide (CH3NH3PbI3−xClx) perovskite films. The data show low yields of spin coated perovskite material (ca. 1\%) and preferential deposition of I− over Cl− in mixed halide films.",

keywords = "Solar energy materials, Thin films, Manufacturing, Perovskites, Composition",

author = "Holliman, \{Peter J.\} and Jones, \{Eurig W.\} and Hobbs, \{Robert J.\} and Arthur Connell and Leo Furnell and Rosie Anthony and Kershaw, \{Christopher P.\}",

year = "2019",

month = jun,

doi = "10.1016/j.mlblux.2019.100011",

language = "English",

volume = "2",

journal = "Materials Letters: X",

issn = "2590-1508",

publisher = "Elsevier BV",

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TY - JOUR

T1 - Quantitative chemical analysis of perovskite deposition using spin coating

AU - Holliman, Peter J.

AU - Jones, Eurig W.

AU - Hobbs, Robert J.

AU - Connell, Arthur

AU - Furnell, Leo

AU - Anthony, Rosie

AU - Kershaw, Christopher P.

PY - 2019/6

Y1 - 2019/6

N2 - Lead and halide ion compositions of spin coated organo-lead halide perovskite films have been quantified using ion chromatography (IC) and atomic absorption spectroscopy (AAS) using perovskite films manufactured by 5 different researchers (3 replicates per treatment) to monitor variability between researchers and individual researcher reproducibility. Planar and mesoporous TiO2-coated glass substrates have been studied along with tribromide (CH3NH3PbBr3), triiodide (CH3NH3PbI3) and mixed halide (CH3NH3PbI3−xClx) perovskite films. The data show low yields of spin coated perovskite material (ca. 1%) and preferential deposition of I− over Cl− in mixed halide films.

AB - Lead and halide ion compositions of spin coated organo-lead halide perovskite films have been quantified using ion chromatography (IC) and atomic absorption spectroscopy (AAS) using perovskite films manufactured by 5 different researchers (3 replicates per treatment) to monitor variability between researchers and individual researcher reproducibility. Planar and mesoporous TiO2-coated glass substrates have been studied along with tribromide (CH3NH3PbBr3), triiodide (CH3NH3PbI3) and mixed halide (CH3NH3PbI3−xClx) perovskite films. The data show low yields of spin coated perovskite material (ca. 1%) and preferential deposition of I− over Cl− in mixed halide films.

KW - Solar energy materials

KW - Thin films

KW - Manufacturing

KW - Perovskites

KW - Composition

U2 - 10.1016/j.mlblux.2019.100011

DO - 10.1016/j.mlblux.2019.100011

M3 - Article

SN - 2590-1508

VL - 2

JO - Materials Letters: X

JF - Materials Letters: X

M1 - 100011

ER -

Quantitative chemical analysis of perovskite deposition using spin coating

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