Novel Chemical Synthesis and Characterization of CeTi2O6 Brannerite
Research output: Contribution to journal › Article › peer-review
Standard Standard
In: Inorganic Chemistry, Vol. 53, No. 13, 07.07.2014, p. 6761-6768.
Research output: Contribution to journal › Article › peer-review
HarvardHarvard
APA
CBE
MLA
VancouverVancouver
Author
RIS
TY - JOUR
T1 - Novel Chemical Synthesis and Characterization of CeTi2O6 Brannerite
AU - Kong, Linggen
AU - Gregg, Daniel J.
AU - Karatchevtseva, Inna
AU - Zhang, Zhaoming
AU - Blackford, Mark G.
AU - Middleburgh, Simon C.
AU - Lumpkin, Gregory R.
AU - Triani, Gerry
PY - 2014/7/7
Y1 - 2014/7/7
N2 - Cerium titanate CeTi2O6 was prepared by a new soft chemistry route in aqueous solution. A suite of characterization techniques, including X-ray diffraction, thermal analysis, vibrational spectroscopy, and scanning and transmission electron spectroscopy, were employed to investigate the brannerite structure formation and its bulk properties. The synthesized powder formed the brannerite crystal structure upon calcination at temperatures as low as 800 degrees C. Samples sintered at 1350 degrees C possess a high level of crystallinity. X-ray absorption near-edge structure results indicate the presence of six-coordinated Ce4+ in the brannerite samples.
AB - Cerium titanate CeTi2O6 was prepared by a new soft chemistry route in aqueous solution. A suite of characterization techniques, including X-ray diffraction, thermal analysis, vibrational spectroscopy, and scanning and transmission electron spectroscopy, were employed to investigate the brannerite structure formation and its bulk properties. The synthesized powder formed the brannerite crystal structure upon calcination at temperatures as low as 800 degrees C. Samples sintered at 1350 degrees C possess a high level of crystallinity. X-ray absorption near-edge structure results indicate the presence of six-coordinated Ce4+ in the brannerite samples.
U2 - 10.1021/ic500563j
DO - 10.1021/ic500563j
M3 - Article
VL - 53
SP - 6761
EP - 6768
JO - Inorganic Chemistry
JF - Inorganic Chemistry
SN - 0020-1669
IS - 13
ER -